Patente
PROCESS FOR PRODUCING STEROL OR STANOL ESTERS BY ENZYMATIC TRANSESTERIFICATION IN SOLVENT AND WATER FREE MEDIA
Registration in:
D00I1096
US2003092096 A1
US 10/205,964
Author
FUENZALIDA-DIAZ, MIGUELITO ANGEL
MARKOVITS-ROJAS, ALEJANDRO
MARKOVITS-SCHERSL, ANDRES
MARTINEZ-BASTERRECHEA, IRENE
Institutions
Abstract
A process for producing steryl or stanyl esters, comprises the steps of:
a) forming a reacting mixture by contacting a lipase with a reactant mixture wherein the reactant mixture comprise sterols or stanols and one or more esters selected from the group consisting of esters of a fatty acid with a short chain aliphatic alcohol;
b) separating the lipase from the reacting mixture to form a reacted mixture; and
c) separating steryl or stanyl esters from the reacted mixture.
The reaction is carried out in stirred reactors at pressures below atmospheric pressure and temperatures from 30 to 90° C. The separation of esters from the reacted mixtures is carried out by distillation at low pressures.
A process for esterifying sterols or stanols comprise forming a reacting mixture by contacting a lipase with a reactant mixture wherein the reactant mixture comprise sterols or stanols and one or more esters selected from the group consisting of esters of a fatty acid with a short chain aliphatic alcohol. The reaction of esterification is carried out in stirred reactors at pressures below atmospheric pressure and temperatures from 30 to 90° C.A process for producing steryl or stanyl esters, comprises the steps of:
a) forming a reacting mixture by contacting a lipase with a reactant mixture wherein the reactant mixture comprise sterols or stanols and one or more esters selected from the group consisting of esters of a fatty acid with a short chain aliphatic alcohol;
b) separating the lipase from the reacting mixture to form a reacted mixture; and
c) separating steryl or stanyl esters from the reacted mixture.
The reaction is carried out in stirred reactors at pressures below atmospheric pressure and temperatures from 30 to 90° C. The separation of esters from the reacted mixtures is carried out by distillation at low pressures.
A process for esterifying sterols or stanols comprise forming a reacting mixture by contacting a lipase with a reactant mixture wherein the reactant mixture comprise sterols or stanols and one or more esters selected from the group consisting of esters of a fatty acid with a short chain aliphatic alcohol. The reaction of esterification is carried out in stirred reactors at pressures below atmospheric pressure and temperatures from 30 to 90° C.A process for producing steryl or stanyl esters, comprises the steps of:
a) forming a reacting mixture by contacting a lipase with a reactant mixture wherein the reactant mixture comprise sterols or stanols and one or more esters selected from the group consisting of esters of a fatty acid with a short chain aliphatic alcohol;
b) separating the lipase from the reacting mixture to form a reacted mixture; and
c) separating steryl or stanyl esters from the reacted mixture.
The reaction is carried out in stirred reactors at pressures below atmospheric pressure and temperatures from 30 to 90° C. The separation of esters from the reacted mixtures is carried out by distillation at low pressures.
A process for esterifying sterols or stanols comprise forming a reacting mixture by contacting a lipase with a reactant mixture wherein the reactant mixture comprise sterols or stanols and one or more esters selected from the group consisting of esters of a fatty acid with a short chain aliphatic alcohol. The reaction of esterification is carried out in stirred reactors at pressures below atmospheric pressure and temperatures from 30 to 90° C.A process for producing steryl or stanyl esters, comprises the steps of:
a) forming a reacting mixture by contacting a lipase with a reactant mixture wherein the reactant mixture comprise sterols or stanols and one or more esters selected from the group consisting of esters of a fatty acid with a short chain aliphatic alcohol;
b) separating the lipase from the reacting mixture to form a reacted mixture; and
c) separating steryl or stanyl esters from the reacted mixture.
The reaction is carried out in stirred reactors at pressures below atmospheric pressure and temperatures from 30 to 90° C. The separation of esters from the reacted mixtures is carried out by distillation at low pressures.
A process for esterifying sterols or stanols comprise forming a reacting mixture by contacting a lipase with a reactant mixture wherein the reactant mixture comprise sterols or stanols and one or more esters selected from the group consisting of esters of a fatty acid with a short chain aliphatic alcohol. The reaction of esterification is carried out in stirred reactors at pressures below atmospheric pressure and temperatures from 30 to 90° C.A process for producing steryl or stanyl esters, comprises the steps of:
a) forming a reacting mixture by contacting a lipase with a reactant mixture wherein the reactant mixture comprise sterols or stanols and one or more esters selected from the group consisting of esters of a fatty acid with a short chain aliphatic alcohol;
b) separating the lipase from the reacting mixture to form a reacted mixture; and
c) separating steryl or stanyl esters from the reacted mixture.
The reaction is carried out in stirred reactors at pressures below atmospheric pressure and temperatures from 30 to 90° C. The separation of esters from the reacted mixtures is carried out by distillation at low pressures.
A process for esterifying sterols or stanols comprise forming a reacting mixture by contacting a lipase with a reactant mixture wherein the reactant mixture comprise sterols or stanols and one or more esters selected from the group consisting of esters of a fatty acid with a short chain aliphatic alcohol. The reaction of esterification is carried out in stirred reactors at pressures below atmospheric pressure and temperatures from 30 to 90° C.A process for producing steryl or stanyl esters, comprises the steps of:
a) forming a reacting mixture by contacting a lipase with a reactant mixture wherein the reactant mixture comprise sterols or stanols and one or more esters selected from the group consisting of esters of a fatty acid with a short chain aliphatic alcohol;
b) separating the lipase from the reacting mixture to form a reacted mixture; and
c) separating steryl or stanyl esters from the reacted mixture.
The reaction is carried out in stirred reactors at pressures below atmospheric pressure and temperatures from 30 to 90° C. The separation of esters from the reacted mixtures is carried out by distillation at low pressures.
A process for esterifying sterols or stanols comprise forming a reacting mixture by contacting a lipase with a reactant mixture wherein the reactant mixture comprise sterols or stanols and one or more esters selected from the group consisting of esters of a fatty acid with a short chain aliphatic alcohol. The reaction of esterification is carried out in stirred reactors at pressures below atmospheric pressure and temperatures from 30 to 90° C. CONCEDIDA