Articulo
Crystal structure of (2R,4S,5R)-2-(4-benzyloxy-5-benzyloxymethyltetrahydrofuranyl) triphenyIphosphoníum tetrafluoroborate tetrachloromethane solvate, C<sub>37</sub>H<sub>36</sub>PBF<sub>4</sub>O</sub>3</sub> CCI<sub>4</sub>
Registro en:
issn:2197-4578
Autor
Frey, W.
Lieberknecht, A.
Griesser, H.
Bravo, Rodolfo Daniel
Colinas, Pedro Alfonso
Grigera, José Raúl
Institución
Resumen
Source of material: The title compound was prepared by reaction of methyl 3,5-di-0-benzyl-2,3-dideoxy-D-ribofuranoside with hydrogentriphenylphosphonium tetrafluoroborate in acetonitrile. The precipitated phosphonium salt was recrystallized from tetrachloromethane/dichloromethane.
One tetrachloromethane solvent molecule per asymmetric unit was found. This solvent molecule was strongly disordered. Centro de Estudios de Compuestos Orgánicos Instituto de Física de Líquidos y Sistemas Biológicos