N-{4-[(2E)-3-(2H-1,3-Benzodioxol-5-yl)prop-2-enoyl]phenyl}quinoline-3-carboxamide

dc.date.accessioned2021-08-23T22:50:39Z
dc.date.accessioned2022-10-19T00:17:20Z
dc.date.available2021-08-23T22:50:39Z
dc.date.available2022-10-19T00:17:20Z
dc.date.created2021-08-23T22:50:39Z
dc.date.issued2017
dc.identifierhttp://hdl.handle.net/10533/250654
dc.identifier1150712
dc.identifierWOS:000424424100003
dc.identifier.urihttps://repositorioslatinoamericanos.uchile.cl/handle/2250/4481917
dc.description.abstractAn amide chalconehas been synthesized in a two-step reaction. First, N-(4-acetylphenyl) quinoline-3-carboxamide 2 was synthesized by the reaction of quinoline-3-carboxylic acid 1 and thionyl chloride (SOCl2), following the addition of 4-aminoacetophenone. Then, a typical Claisen-Schmidtreactionwas made between 2 and piperonal using KOH solution as a catalystin ethanol, under ultrasonic irradiation. The structure of the target compound was established by FTIR (Fourier-transform infrared spectroscopy), HRMS, H-1 and C-13-NMR.
dc.languageeng
dc.relationhttps://doi.org/10.3390/M960
dc.relationhandle/10533/111557
dc.relation10.3390/M960
dc.relationhandle/10533/111541
dc.relationhandle/10533/108045
dc.rightsinfo:eu-repo/semantics/article
dc.rightsinfo:eu-repo/semantics/openAccess
dc.rightsAtribución-NoComercial-SinDerivadas 3.0 Chile
dc.rightshttp://creativecommons.org/licenses/by-nc-nd/3.0/cl/
dc.titleN-{4-[(2E)-3-(2H-1,3-Benzodioxol-5-yl)prop-2-enoyl]phenyl}quinoline-3-carboxamide
dc.typeArticulo


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