Complete 1H and 13C NMR spectral assignment of hydrogenated oxoisoaporphine derivatives

dc.creatorSobarzo Sánchez, Eduardo
dc.creatorCassels Niven, Bruce
dc.creatorCastedo, Luis
dc.date.accessioned2018-12-20T14:26:58Z
dc.date.available2018-12-20T14:26:58Z
dc.date.created2018-12-20T14:26:58Z
dc.date.issued2003
dc.identifierMagnetic Resonance in Chemistry, Volumen 41, Issue 7, 2018, Pages 545-548
dc.identifier07491581
dc.identifier10.1002/mrc.1205
dc.identifierhttps://repositorio.uchile.cl/handle/2250/156067
dc.description.abstract2,3,8,9,10,11-Hexahydro-7H-dibenzo[de,h]quinolin-7-one, 5-methoxy-2,3,8,9,10,11-hexahydro-7H-dibenzo[de,h] quinolin-7-one, 5-methoxy-6-hydroxy-1,2,3,7a,8,9,10,11, 11a,11b-decahydro-7H-dibenzo[de,h]quinolin-7-one, 5-methoxy-5,6,8,9,10,11-hexahydro-4H-dibenzo[de,h]quinolin-7-ol, 5,6,8,9,10,11-hexahydro-4H-dibenzo[de,h]quinolin-7-ol and 5,6-dihydro-4H-dibenzo[de,h]quinolin-7-ol were prepared by catalytic hydrogenation of oxoisoaporphines or their 2,3-dihydro derivatives over PtO 2 in acetic acid under mild conditions. Their structures were confirmed and 1H and 13C NMR spectra were completely assigned using a combination of one- and two-dimensional NMR techniques. Copyright © 2003 John Wiley & Sons, Ltd.
dc.languageen
dc.rightshttp://creativecommons.org/licenses/by-nc-nd/3.0/cl/
dc.rightsAttribution-NonCommercial-NoDerivs 3.0 Chile
dc.sourceMagnetic Resonance in Chemistry
dc.subject4H-dibenzo[de,h]quinolin-7-ol
dc.subject7H-dibenzo[de,h]quinolin-7-one
dc.subject13C NMR
dc.subject1H NMR
dc.subject1H-1H COSY
dc.subjectHMBC
dc.subjectHMQC
dc.subjectNMR
dc.titleComplete 1H and 13C NMR spectral assignment of hydrogenated oxoisoaporphine derivatives
dc.typeArtículo de revista


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