Artículos de revistas
Assessment Of Robustness On Analysis Using Headspace Solid-phase Microextraction And Comprehensive Two-dimensional Gas Chromatography Through Experimental Designs
Registro en:
Talanta. Elsevier, v. 129, n. , p. 303 - 308, 2014.
399140
10.1016/j.talanta.2014.05.038
2-s2.0-84903157175
Autor
Oliveira L.F.
Braga S.C.G.N.
Filgueiras P.R.
Augusto F.
Poppi R.J.
Institución
Resumen
Plackett-Burman experimental design was applied for the robustness assessment of GC×GC-qMS (Comprehensive Two-Dimensional Gas Chromatography with Fast Quadrupolar Mass Spectrometric Detection) in quantitative and qualitative analysis of volatiles compounds from chocolate samples isolated by headspace solid-phase microextraction (HS-SPME). The influence of small changes around the nominal level of six factors deemed as important on peak areas (carrier gas flow rate, modulation period, temperature of ionic source, MS photomultiplier power, injector temperature and interface temperature) and of four factors considered as potentially influential on spectral quality (minimum and maximum limits of the scanned mass ranges, ions source temperature and photomultiplier power). The analytes selected for the study were 2,3,5-trimethylpyrazine, 2-octanone, octanal, 2-pentyl-furan, 2,3,5,6-tetramethylpyrazine, and 2-nonanone e nonanal. The factors pointed out as important on the robustness of the system were photomultiplier power for quantitative analysis and lower limit of mass scanning range for qualitative analysis. © 2014 Elsevier B.V. 129
303 308 (2005) Guidelines Prepared Within the International Conference on Harmonisation of Technical Requirements for the Registration of Pharmaceuticals for Human Use (ICH), Validation of Analytical Procedures: Text and Methodology, Q2(R1), p. 5. , http://www.ich.org/ Adouani, I., Du, M., Hang, T., (2013) Chromatographia, 76, pp. 499-508 Kahsay, G., Shraim, F., Villatte, P., Rotger, J., Cassus-Coussere, C., Schepdael, A.V., Hoogmartens, J., Adams, E., (2013) J. Pharm. Biomed. Anal., 75, pp. 199-206 Vasconcelos De Sá, L.R., De Oliveira, M.A.L., Cammarota, M.C., Matos, A., Ferreira-Leitão, V.S., (2011) Int. J. Hydrog. Energy, 36, pp. 15177-15186 Gomes, F.P., Garcia, P.L., (2012) Talanta, 101, pp. 495-503 Marák, J., Stanová, A., Vaváková, V., Hrenáková, M., Kaniansky, D., (2012) J. Chromatogr. A, 1267, pp. 252-258 Neumajer, G., Sohajda, T., Darcsi, A., Tóth, G., Szente, L., Noszál, B., Béni, S., (2012) J. Pharm. Biomed. Anal., 62, pp. 42-47 Pizarro, C., Martínez-Uruñuela, A., Pérez-Del-Notario, N., González-Sáiz, J.M., (2008) J. Chromatogr. A, 1208, pp. 54-61 Stefanelli, P., Generali, T., Girolimetti, S., Bardini, D.A., (2013) Accredit. Qual. Assur., 18, pp. 313-322 Nevado, J.J.B., Llerena, M.J.V., Cabanillas, C.G., Robledo, V.R., (2006) J. Chromatogr. A, 1123, pp. 130-133 Gaujac, A., Dempster, N., Navickiene, S., Brandt, S.D., De Andrade, J.B., (2013) Talanta, 106, pp. 394-398 Uçaktürk, E., (2013) J. Pharm. Biomed. Anal., 74, pp. 71-76 Liu, Z., Phillips, J.B., (1991) J. Chromatogr. Sci., 29, pp. 227-231 Seeley, J.V., Seeley, S.K., (2013) Anal. Chem., 85, pp. 557-578 Adahchour, M., Beens, J., Brinkman, U.A.Th., (2008) J. Chromatogr. A, 1186, pp. 67-108 Marriott, P.J., Chin, S., Maikhunthod, B., Schmarr, H., Bieri, S., (2012) Trends Anal. Chem., 34, pp. 1-21 Zeng, Z., Hugel, H.M., Marriott, P.J., (2011) Anal. Bioanal. Chem., 401, pp. 2373-2386 Nizio, K.D., Harynuk, J.J., (2012) J. Chromatogr. A, 1252, pp. 171-176 Tranchida, P.Q., Zoccali, M., Bonaccorsi, I., Dugo, P., Mondello, L., Dugo, G., (2013) J. Chromatogr. A, 1305, pp. 276-284 Ryan, D., Shellie, R., Tranchida, P., Casilli, A., Mondello, L., Marriott, P., (2004) J. Chromatogr. A, 1054, pp. 57-65 Rivellino, S.R., Hantao, L.W., Risticevic, S., Carasek, E., Pawliszyn, J., Augusto, F., (2013) Food Chem., 141, pp. 1828-1833 Williams, A., Ryan, D., Guasca, A.O., Marriott, P., Pang, E., (2005) J. Chromatogr. B, 817, pp. 97-107 Hantao, L.W., Toledo, B.R., Ribeiro, F.A.L., Pizetta, M., Pierozzi, C.G., Furtado, E.L., Augusto, F., (2013) Talanta, 116, pp. 1079-1084 Mostafa, A., Edwards, M., Górecki, T., (2012) J. Chromatogr. A, 1255, pp. 38-55 Dejaegher, B., Heyden, Y.V., (2007) J. Chromatogr. A, 1158, pp. 138-157 Nijhuis, A., Van Der Knaap, H.C.M., De Jong, S., Vandeginste, B.G.M., (1999) Anal. Chim. Acta, 391, pp. 187-202 Vander Heyden, Y., Nijhuis, A., Smeyers-Verbeke, J., Vandeginste, B.G.M., Massart, D.L., (2001) J. Pharm. Biomed. Anal., 24, pp. 723-753 Dejaegher, B., Heyden, Y.V., (2011) J. Pharm. Biomed., 56, pp. 141-158 Plackett, R.L., Burman, J.P., (1964) Biometrika, 33, pp. 305-325 (2013) Anal. Methods, 5, pp. 1901-1903. , Analytical Methods Committee Dong, F., (1993) Stat. Sin., 3, pp. 209-217 Oliveira, A.M., Pereira, N.R., Marsaioli Junior, A., Augusto, F., (2004) J. Chromatogr. A, 1025, pp. 115-124 Pini, G.F., Brito, E.S., García, N.H.P., Valente, A.L.P., Augusto, F., (2004) J. Braz. Chem. Soc., 15, pp. 267-271 Bruns, R.E., Scarminio, I.S., Neto, B.B., (2006) Statistical Design - Chemometrics, , first ed. Elsevier Netherlands Photomultiplier Tubes: Construction and Operating Characteristics/ Connections to External Circuits, , Hamamatsu Photonics K.K. Shizuoka-ken, Japan