Assessment Of Robustness On Analysis Using Headspace Solid-phase Microextraction And Comprehensive Two-dimensional Gas Chromatography Through Experimental Designs

dc.creatorOliveira L.F.
dc.creatorBraga S.C.G.N.
dc.creatorFilgueiras P.R.
dc.creatorAugusto F.
dc.creatorPoppi R.J.
dc.date2014
dc.date2015-06-25T18:01:04Z
dc.date2015-11-26T14:56:39Z
dc.date2015-06-25T18:01:04Z
dc.date2015-11-26T14:56:39Z
dc.date.accessioned2018-03-28T22:08:36Z
dc.date.available2018-03-28T22:08:36Z
dc.identifier
dc.identifierTalanta. Elsevier, v. 129, n. , p. 303 - 308, 2014.
dc.identifier399140
dc.identifier10.1016/j.talanta.2014.05.038
dc.identifierhttp://www.scopus.com/inward/record.url?eid=2-s2.0-84903157175&partnerID=40&md5=9e734f24c6070bca7f64dd4b80ddfba1
dc.identifierhttp://www.repositorio.unicamp.br/handle/REPOSIP/87488
dc.identifierhttp://repositorio.unicamp.br/jspui/handle/REPOSIP/87488
dc.identifier2-s2.0-84903157175
dc.identifier.urihttp://repositorioslatinoamericanos.uchile.cl/handle/2250/1255499
dc.descriptionPlackett-Burman experimental design was applied for the robustness assessment of GC×GC-qMS (Comprehensive Two-Dimensional Gas Chromatography with Fast Quadrupolar Mass Spectrometric Detection) in quantitative and qualitative analysis of volatiles compounds from chocolate samples isolated by headspace solid-phase microextraction (HS-SPME). The influence of small changes around the nominal level of six factors deemed as important on peak areas (carrier gas flow rate, modulation period, temperature of ionic source, MS photomultiplier power, injector temperature and interface temperature) and of four factors considered as potentially influential on spectral quality (minimum and maximum limits of the scanned mass ranges, ions source temperature and photomultiplier power). The analytes selected for the study were 2,3,5-trimethylpyrazine, 2-octanone, octanal, 2-pentyl-furan, 2,3,5,6-tetramethylpyrazine, and 2-nonanone e nonanal. The factors pointed out as important on the robustness of the system were photomultiplier power for quantitative analysis and lower limit of mass scanning range for qualitative analysis. © 2014 Elsevier B.V.
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dc.languageen
dc.publisherElsevier
dc.relationTalanta
dc.rightsfechado
dc.sourceScopus
dc.titleAssessment Of Robustness On Analysis Using Headspace Solid-phase Microextraction And Comprehensive Two-dimensional Gas Chromatography Through Experimental Designs
dc.typeArtículos de revistas


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