dc.contributorUniversidade Estadual Paulista (UNESP)
dc.creatorSaleh, Mayra A D
dc.creatorPadilha, Pedro M.
dc.creatorHauptli, Lucélia
dc.creatorBerto, Dirlei A.
dc.date2015-12-07T15:32:01Z
dc.date2016-10-25T21:22:50Z
dc.date2015-12-07T15:32:01Z
dc.date2016-10-25T21:22:50Z
dc.date2015
dc.date.accessioned2017-04-06T09:27:50Z
dc.date.available2017-04-06T09:27:50Z
dc.identifierJournal Of Animal Science And Biotechnology, v. 6, n. 1, p. 6-32, 2015.
dc.identifier1674-9782
dc.identifierhttp://hdl.handle.net/11449/131146
dc.identifierhttp://acervodigital.unesp.br/handle/11449/131146
dc.identifier10.1186/s40104-015-0030-3
dc.identifier26244092
dc.identifierPMC4523951
dc.identifierhttp://dx.doi.org/10.1186/s40104-015-0030-3
dc.identifier.urihttp://repositorioslatinoamericanos.uchile.cl/handle/2250/941686
dc.descriptionA sample preparation method based on ultrasound assisted-extraction (UAE) of Ca, Mg and P from swine feed has been described. The experiment was performed to cover the variables influencing the sonication process and, the method validation using standard reference material. Final solutions obtained upon sonication were analyzed by flame atomic absorption spectrometry (for Ca and Mg) and by UV-vis spectrophotometry (for P). The best conditions for metal extraction were as follows: sample mass: 100 mg in 20 mL 0.10 mol/L HCl, a particle size: <60 μm, sonication time: 5 cycles of 10 s and ultrasound power: 102 W. The UAE method was applied in digestibility assays in different piglet feeds and their results showed that it is highly comparable (P > 0.05) to the other methods used for such purposes, as block digestion, and offered a Ca, Mg and P method of quantification limit of 10.6, 12.4 and 14 mg/kg, respectively. The major advantages of the UAE method compared to other methods are the high treatment rate, low reagent usage in the extracts and, it does not generate toxic residues that might negatively affect human health and the environment, accompanied by good precision and accuracy.
dc.languageeng
dc.publisherJournal Of Animal Science And Biotechnology
dc.relationJournal Of Animal Science And Biotechnology
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectDigestibility assay
dc.subjectGreen analytical chemistry
dc.subjectMacronutrients
dc.subjectPiglet
dc.subjectUltrasound-assisted extraction
dc.titleThe ultra-sonication of minerals in swine feed
dc.typeOtro


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