dc.contributorUniversidade Estadual Paulista (UNESP)
dc.creatorRibeiro, M. L.
dc.creatorAmador, JR
dc.creatorPolese, L.
dc.creatorJardim, EFG
dc.creatorMinelli, E. V.
dc.creatorde Cordis, OCP
dc.date2014-05-20T15:24:01Z
dc.date2016-10-25T17:58:04Z
dc.date2014-05-20T15:24:01Z
dc.date2016-10-25T17:58:04Z
dc.date2000-07-01
dc.date.accessioned2017-04-05T23:44:54Z
dc.date.available2017-04-05T23:44:54Z
dc.identifierJournal of Agricultural and Food Chemistry. Washington: Amer Chemical Soc, v. 48, n. 7, p. 2818-2820, 2000.
dc.identifier0021-8561
dc.identifierhttp://hdl.handle.net/11449/34674
dc.identifierhttp://acervodigital.unesp.br/handle/11449/34674
dc.identifier10.1021/jf990380b
dc.identifierWOS:000088319600034
dc.identifierhttp://dx.doi.org/10.1021/jf990380b
dc.identifier.urihttp://repositorioslatinoamericanos.uchile.cl/handle/2250/878549
dc.descriptionAn efficient analytical method is described for the analysis of dicofol residues in pulp and orange peel. Samples are mixed with Celite and transferred to chromatographic columns prepacked with silica gel. Dicofol is eluted with ethyl acetate, and the extracts are analyzed by gas chromatography with electron capture detection. Mean recoveries for dicofol at levels of 0.5, 2.0, 5.0, and 10 mg/kg ranged from 87 to 95% with relative standard deviation values between 2.6 and 9.0%. To investigate the effect of a pilot washing system on dicofol residues in oranges, the analytical procedure was applied to samples submitted to different treatments with commercial formulations under field and laboratory conditions. The orange samples with and without washing were analyzed in duplicate, and the results indicated that washing under the described conditions did not allow a complete removal of dicofol residues from orange peel.
dc.languageeng
dc.publisherAmer Chemical Soc
dc.relationJournal of Agricultural and Food Chemistry
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectdicofol residues
dc.subjectgas chromatography
dc.subjectorange
dc.subjectwashing
dc.titleEffect of a pilot washing system on dicofol levels in orange matrix
dc.typeOtro


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