Otro
Formation of SnO2 supported porous membranes
Registro en:
Journal of Sol-gel Science and Technology. Dordrecht: Kluwer Academic Publ, v. 8, n. 1-3, p. 477-481, 1997.
0928-0707
10.1007/BF02436885
WOS:A1997WQ33400076
Autor
Santos, LRB
Pulcinelli, Sandra Helena
Santilli, Celso Valentim
Resumen
In this work, the effect of the substrate microstructure on the formation of SnO2 membranes and of the sintering conditions on their porosity have been analysed. Samples have been prepared by colloidal suspensions cast on alumina or kaolin substrates. Supported membranes have been characterized by Hg porosimetry, MEV, XRD and N-2 adsorption-desorption isotherms. The results show that the narrower pore size distribution of alumina substrate allowed to prepare membranes more homogeneous and free of cracks than that supported on kaolin. The crystallite and pore sizes of the membranes could be controlled by adjusting the temperature of sintering, allowing materials with adequate microstructure with application for ultrafiltration process.