Development and validation of the quantitative analysis of cefuroxime sodium in powder for injection by infrared spectroscopy

dc.contributorUniversidade Estadual Paulista (Unesp)
dc.creatorVieira, Daniela Cristina de Macedo [UNESP]
dc.creatorSalgado, Hérida Regina Nunes [UNESP]
dc.date2016-01-28T16:56:37Z
dc.date2016-01-28T16:56:37Z
dc.date2012
dc.date.accessioned2023-09-12T08:16:41Z
dc.date.available2023-09-12T08:16:41Z
dc.identifierhttp://dx.doi.org/10.5923/j.pc.20120201.02
dc.identifierAdvances in Analytical Chemistry, v. 2, n. 6, p. 80-87, 2012.
dc.identifier2163-2847
dc.identifierhttp://hdl.handle.net/11449/133791
dc.identifier10.5923/j.pc.20120201.02
dc.identifier6438813160518299
dc.identifier9881720291571774
dc.identifier.urihttps://repositorioslatinoamericanos.uchile.cl/handle/2250/8783043
dc.descriptionCeftazidime quantification by the infrared spectroscopy was developed and validated for pharmaceutical preparations in powder for injection. This method involved absorbance measurements of the band corresponding to aromatic ring centered by 1475-1600 cm-1. Selectivity, linearity, precision and accuracy were determined in order to validate the proposed method. It was also found that the excipient did not interfere with the assay. Calibration curve was obtained for ceftazidime at 0.5 to 7.0 mg, and mean recovery percentage was 98.98 ± 0.70. The proposed method was successfully applied to the assay of ceftazidime in powder for injection.
dc.descriptionFundação para o Desenvolvimento da UNESP (FUNDUNESP)
dc.descriptionFundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
dc.descriptionConselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)
dc.descriptionUniversidade Estadual Paulista Júlio de Mesquita Filho, Departamento de Farmacos e Médicamentos, Faculdade de Ciências Farmacêuticas de Araraquara, Araraquara, Rodovia Araraquara-Jaú, km1, Campus, CEP 14801-902, SP, Brasil
dc.descriptionUniversidade Estadual Paulista Júlio de Mesquita Filho, Departamento de Farmacos e Médicamentos, Faculdade de Ciências Farmacêuticas de Araraquara, Araraquara, Rodovia Araraquara-Jaú, km1, Campus, CEP 14801-902, SP, Brasil
dc.format80-87
dc.languageeng
dc.publisherScientific & Academic Publishing
dc.relationAdvances in Analytical Chemistry
dc.rightsAcesso restrito
dc.sourceCurrículo Lattes
dc.subjectCeftazidime
dc.subjectInfrared
dc.subjectSpectroscopy
dc.subjectQuantitative
dc.subjectDetermination
dc.titleDevelopment and validation of the quantitative analysis of cefuroxime sodium in powder for injection by infrared spectroscopy
dc.typeArtigo


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