Síntesis electroquímica de películas de polipirrol-porfirina modificadas con puntos de carbono y evaluación de sus propiedades como supercapacitor

dc.contributorCortés Montañez, María Teresa
dc.contributorLizcano Valbuena, William Hernando
dc.contributorMoreno Piraján, Juan Carlos
dc.contributorGrupo de electroquímica
dc.creatorMoreno Gualtero, Cristian Camilo
dc.date.accessioned2023-01-27T15:33:49Z
dc.date.accessioned2023-09-07T00:38:51Z
dc.date.available2023-01-27T15:33:49Z
dc.date.available2023-09-07T00:38:51Z
dc.date.created2023-01-27T15:33:49Z
dc.date.issued2022-12-01
dc.identifierhttp://hdl.handle.net/1992/64288
dc.identifierinstname:Universidad de los Andes
dc.identifierreponame:Repositorio Institucional Séneca
dc.identifierrepourl:https://repositorio.uniandes.edu.co/
dc.identifier.urihttps://repositorioslatinoamericanos.uchile.cl/handle/2250/8727585
dc.description.abstractPelículas de polipirrol (PPy) se sintetizaron a través del método de pulsos galvanostáticos haciendo uso de diferentes dopantes y co-dopantes: ácido p-toluensulfónico (pTS), 5,10,15,20-tetrakis(4-sulfonatofenil)porfirina (TPPS), su complejo de Cu(II) (CuTPPS) y puntos de carbono (CD) para evaluar la influencia de estos compuestos en las propiedades de carga del material resultante. Las técnicas utilizadas para evaluar el desempeño electroquímico fueron la voltametría cíclica (CV), ciclos galvanostáticos de carga y descarga (GCD) y espectroscopía de impedancia electroquímica (EIS); se realizaron ensayos de cronoamperometría (CA) para determinar el área electroactiva de las películas sintetizadas.
dc.description.abstractPolypyrrole (PPy) films were synthesized through galvanostatic pulse method with different dopants and co-dopants: p-toluenesulfonic acid (pTS), 5,10,15,20- tetrakis(4-sulfonatophenyl)porphyrin (TPPS), its Cu (II) complex (CuTPPS) and carbon dots (CD) to evaluate the influence of these compounds on the charge properties of the materials. The techniques used to evaluate electrochemical performance were cyclic voltammetry (CV), galvanostatic charge and discharge (GCD) and electrochemical impedance spectroscopy (EIS). Additionally, observations were made through scanning electron microscopy (SEM) in order to determine morphological variations of the materials. The specific capacitances obtained were: PPy/PTSA/TPPS: 244 F/g; PPy/PTSA/CuTPPS: 237 F/g; PPy/PTSA/CuTPPS: 298 F/g y PPy/PTSA/CuTPPS/CD: 335 F/g at 0.5 mA/cm2 . The capacitance retention was performed through the GCD technique at 5 mA/cm2 , which did not show significant variation in the systems: PPy/PTSA/TPPS 92% up to 3000 cycles PPy/PTSA/CuTPPS: 99% up to 2000 cycles; PPy/ PTSA /TPPS/CD: 89% up to 3000 cycles and PPy/PTSA/CuTPPS/CD: 98% up to 2000 cycles.
dc.languagespa
dc.publisherUniversidad de los Andes
dc.publisherMaestría en Química
dc.publisherFacultad de Ciencias
dc.publisherDepartamento de Química
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dc.rightsAttribution-NonCommercial-NoDerivatives 4.0 Internacional
dc.rightshttp://creativecommons.org/licenses/by-nc-nd/4.0/
dc.rightsinfo:eu-repo/semantics/openAccess
dc.rightshttp://purl.org/coar/access_right/c_abf2
dc.titleSíntesis electroquímica de películas de polipirrol-porfirina modificadas con puntos de carbono y evaluación de sus propiedades como supercapacitor
dc.typeTrabajo de grado - Maestría


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