dc.contributorUniversidade Estadual Paulista (UNESP)
dc.creatorde Aragao, Bernardo J. G.
dc.creatorMessaddeq, Younes
dc.date2014-05-20T14:20:21Z
dc.date2016-10-25T17:41:34Z
dc.date2014-05-20T14:20:21Z
dc.date2016-10-25T17:41:34Z
dc.date2008-01-01
dc.date.accessioned2017-04-05T22:34:01Z
dc.date.available2017-04-05T22:34:01Z
dc.identifierJournal of The Brazilian Chemical Society. São Paulo: Soc Brasileira Quimica, v. 19, n. 8, p. 1582-1594, 2008.
dc.identifier0103-5053
dc.identifierhttp://hdl.handle.net/11449/26118
dc.identifierhttp://acervodigital.unesp.br/handle/11449/26118
dc.identifier10.1590/S0103-50532008000800019
dc.identifierS0103-50532008000800019
dc.identifierWOS:000261658800019
dc.identifierhttp://dx.doi.org/10.1590/S0103-50532008000800019
dc.identifier.urihttp://repositorioslatinoamericanos.uchile.cl/handle/2250/870928
dc.descriptionReliable spectral analysis is only achieved if the spectrum is thoroughly investigated in regard to all hidden and overlapped peaks. This paper describes the steps undertaken to find and separate such peaks in the range of 3000 to 4000 cm(-1) in the case of three different infrared absorption spectra of the glass surface of hydrolyzed silica optical fibers. Peak finding was done by the analysis of the second and fourth derivatives of the digital data, coupled with the available knowledge of infrared spectroscopy of silica-water interaction in the investigated range. Peak separation was accomplished by curve fitting with four different models. The model with the best fit was described by a sum of pure Gaussian peaks. Shoulder limit and detection limit maps were used to validate the revealed spectral features.
dc.languageeng
dc.publisherSoc Brasileira Quimica
dc.relationJournal of the Brazilian Chemical Society
dc.rightsinfo:eu-repo/semantics/openAccess
dc.subjectFTIR
dc.subjectsilica
dc.subjectwater
dc.subjectpeak separation
dc.subjectcurve fitting
dc.titlePeak Separation by Derivative Spectroscopy Applied to FTIR Analysis of Hydrolized Silica
dc.typeOtro


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