dc.contributorUniversidade Estadual Paulista (UNESP)
dc.creatorUgucione, Cássia
dc.creatorGomes Neto, José de Anchieta
dc.creatorCardoso, Arnaldo Alves
dc.date2014-05-20T14:19:35Z
dc.date2016-10-25T17:41:09Z
dc.date2014-05-20T14:19:35Z
dc.date2016-10-25T17:41:09Z
dc.date2002-05-01
dc.date.accessioned2017-04-05T22:31:47Z
dc.date.available2017-04-05T22:31:47Z
dc.identifierQuímica Nova. Sociedade Brasileira de Química, v. 25, n. 3, p. 352-357, 2002.
dc.identifier0100-4042
dc.identifierhttp://hdl.handle.net/11449/25904
dc.identifierhttp://acervodigital.unesp.br/handle/11449/25904
dc.identifier10.1590/S0100-40422002000300003
dc.identifierS0100-40422002000300003
dc.identifierS0100-40422002000300003.pdf
dc.identifierhttp://dx.doi.org/10.1590/S0100-40422002000300003
dc.identifier.urihttp://repositorioslatinoamericanos.uchile.cl/handle/2250/870735
dc.descriptionAn alternative analytical method for nitrogen dioxide (NO2) in atmosphere was developed. The collection of NO2 is performed by a Sep-Pack C-18 cartridge impregnated with 11% (v/v) of triethanolamine plus 3,6 % (v/v) of ethylene glycol plus 25 % (v/v) of acetone combined solution. When the impregnating is used, NO2 is collected with good repeatibility (CV = 3,3 %). The NO2 absorbed in the sampler was stripped from the sorbent with a methanol 5% (v/v) aqueous solution and was determined by colorimetry as nitrite by using the Griess-Saltzman reagent. The detection limit of 1,4 ppb for 60 min sampling at 0,5 L min-1 flow rate was obtained. Preparation and conditioning procedures for TEA-C-18 cartridge, sampling flow rate, absorption capacity and interference of other species are discussed.
dc.descriptionFundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP)
dc.descriptionConselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq)
dc.languagepor
dc.publisherSociedade Brasileira de Química
dc.relationQuímica Nova
dc.rightsinfo:eu-repo/semantics/openAccess
dc.subjectnitrogen dioxide
dc.subjecttriethanolamine
dc.subjectGriess Saltzman reagent
dc.titleMétodo colorimétrico para determinação de dióxido de nitrogênio atmosférico com preconcentração em coluna de c-18
dc.typeOtro


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