dc.contributorUniversidade de São Paulo (USP)
dc.contributorUniv Fed Rio Grande Norte
dc.contributorUniversidade Estadual Paulista (Unesp)
dc.date.accessioned2020-12-10T16:29:32Z
dc.date.accessioned2022-12-19T19:53:37Z
dc.date.available2020-12-10T16:29:32Z
dc.date.available2022-12-19T19:53:37Z
dc.date.created2020-12-10T16:29:32Z
dc.date.issued2000-01-01
dc.identifierQuimica Nova. Sao Paulo: Soc Brasileira Quimica, v. 23, n. 1, p. 113-115, 2000.
dc.identifier0100-4042
dc.identifierhttp://hdl.handle.net/11449/194545
dc.identifierWOS:000085390300020
dc.identifier.urihttps://repositorioslatinoamericanos.uchile.cl/handle/2250/5375181
dc.description.abstractThe effects of the heating rate on a TG curve of a sample have been widely discussed in the literature. This paper shows the influence of heating rate (beta) in thermogravimetry results when stoichiometry determinations are studied. For this purpose the compound Sm(CH3SO3)(3). 2(3-picNO) was considered beta of 2,5; 5; 10; 20 and 40 degrees C min(-1) in dynamic air atmosphere were obtained. The results are in agreement with proposed stoichiometry for beta equal to 2,5 and 5 degrees C min(-1). However, using a higher beta the same results were not obtained resulting in false stoichiometry determinations.
dc.languagepor
dc.publisherSoc Brasileira Quimica
dc.relationQuimica Nova
dc.sourceWeb of Science
dc.subjectheating rate
dc.subjectthermogravimetry
dc.subjectstoichiometry determination
dc.titleIlustration of the influence of the heating rate in thermogravimetry results.
dc.typeArtículos de revistas


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