dc.contributor | Universidade de São Paulo (USP) | |
dc.contributor | Univ Fed Rio Grande Norte | |
dc.contributor | Universidade Estadual Paulista (Unesp) | |
dc.date.accessioned | 2020-12-10T16:29:32Z | |
dc.date.accessioned | 2022-12-19T19:53:37Z | |
dc.date.available | 2020-12-10T16:29:32Z | |
dc.date.available | 2022-12-19T19:53:37Z | |
dc.date.created | 2020-12-10T16:29:32Z | |
dc.date.issued | 2000-01-01 | |
dc.identifier | Quimica Nova. Sao Paulo: Soc Brasileira Quimica, v. 23, n. 1, p. 113-115, 2000. | |
dc.identifier | 0100-4042 | |
dc.identifier | http://hdl.handle.net/11449/194545 | |
dc.identifier | WOS:000085390300020 | |
dc.identifier.uri | https://repositorioslatinoamericanos.uchile.cl/handle/2250/5375181 | |
dc.description.abstract | The effects of the heating rate on a TG curve of a sample have been widely discussed in the literature. This paper shows the influence of heating rate (beta) in thermogravimetry results when stoichiometry determinations are studied. For this purpose the compound Sm(CH3SO3)(3). 2(3-picNO) was considered beta of 2,5; 5; 10; 20 and 40 degrees C min(-1) in dynamic air atmosphere were obtained. The results are in agreement with proposed stoichiometry for beta equal to 2,5 and 5 degrees C min(-1). However, using a higher beta the same results were not obtained resulting in false stoichiometry determinations. | |
dc.language | por | |
dc.publisher | Soc Brasileira Quimica | |
dc.relation | Quimica Nova | |
dc.source | Web of Science | |
dc.subject | heating rate | |
dc.subject | thermogravimetry | |
dc.subject | stoichiometry determination | |
dc.title | Ilustration of the influence of the heating rate in thermogravimetry results. | |
dc.type | Artículos de revistas | |