A competição entre as reações de Clarke-Eschweiler e Pictet-Spengler em fluxo sequencial de plugues

Spano, Michael Brandon Schroder

Brasil | bachelorThesis

dc.contributor	Haminiuk, Charles Windson Isidoro
dc.contributor	Oliveira, Alfredo Ricardo Marques de
dc.contributor	Pilissão, Cristiane
dc.contributor	Rodrigues, Paula Cristina
dc.contributor	Haminiuk, Charles Windson Isidoro
dc.contributor	Oliveira, Alfredo Ricardo Marques de
dc.creator	Spano, Michael Brandon Schroder
dc.date.accessioned	2020-11-11T19:08:22Z
dc.date.accessioned	2022-12-06T14:32:08Z
dc.date.available	2020-11-11T19:08:22Z
dc.date.available	2022-12-06T14:32:08Z
dc.date.created	2020-11-11T19:08:22Z
dc.date.issued	2017-06-23
dc.identifier	SPANO, Michael Brandon Schroder. A competição entre as reações de Clarke-Eschweiler e Pictet-Spengler em fluxo sequencial de plugues. 2017. 64 f. Trabalho de Conclusão de Curso (Graduação em Química) - Universidade Tecnológica Federal do Paraná, Curitiba, 2017.
dc.identifier	http://repositorio.utfpr.edu.br/jspui/handle/1/9139
dc.identifier.uri	https://repositorioslatinoamericanos.uchile.cl/handle/2250/5251037
dc.description.abstract	Herein is described the syntheses of 2-phenylethylamine and homoveratrylamine. The former was used to study the competition between the Clarke-Eschweiler and Pictet-Spengler reactions using segmented plug flow. A flow chemistry system was built around an arduino compatible microcontroller. Syringe pumps were constructed using a 3D printer. The following conditions were tested using sequential plug flow: temperature of 70 °C and 100 °C; and reaction times of 1 min, 5 min and 10 min. The main product observed from sequential plug flow was N,N-dimethyl-2-phenylethylamine when the temperature was 100 °C and reaction time was 1 minute. Pictet-Spengler type products were not observed for the reaction with 2-phenylethylamine as was expected.
dc.publisher	Universidade Tecnológica Federal do Paraná
dc.publisher	Curitiba
dc.publisher	Brasil
dc.publisher	Bacharelado em Química
dc.publisher	UTFPR
dc.rights	openAccess
dc.subject	Síntese orgânica
dc.subject	Análise por injeção de fluxo
dc.subject	Arduino (Controlador programável)
dc.subject	Formaldeído
dc.subject	Química
dc.subject	Organic compounds - Synthesis
dc.subject	Flow injection analysis
dc.subject	Arduino (Programmable controller)
dc.subject	Formaldehyde
dc.subject	Chemistry
dc.title	A competição entre as reações de Clarke-Eschweiler e Pictet-Spengler em fluxo sequencial de plugues
dc.type	bachelorThesis

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Universidade Tecnológica Federal do Paraná (Brasil)