| dc.creator | Silva, Maitê Medeiros de Santana | |
| dc.creator | Sena, Michael Segundo | |
| dc.creator | Moriyama, André Luis Lopes | |
| dc.creator | Souza, Carlson Pereira de | |
| dc.creator | Santos, A. G. | |
| dc.date | 2021-04-28T20:34:28Z | |
| dc.date | 2018-10-01 | |
| dc.identifier | SILVA, M.M.S. ; SENA, M.S. ; LOPES-MORIYAMA, A.L. ; SOUZA, C.P. ; SANTOS, A.G. . Experimental Planning of the Synthesis of Strontium Molybdate by EDTA-Citrate and its Structural Influence, Morphology and Optical Bandgap. CERAMICS INTERNATIONAL, v. 44, p. 16606-16614, 2018. Disponível em: https://www.sciencedirect.com/science/article/pii/S0272884218315165?via%3Dihub#!. Acesso em: 28 abr. 2021. https://doi.org/10.1016/j.ceramint.2018.06.087 | |
| dc.identifier | 0272-8842 | |
| dc.identifier | https://repositorio.ufrn.br/handle/123456789/32339 | |
| dc.identifier | 10.1016/j.ceramint.2018.06.087 | |
| dc.description | It was initially used a 23 experimental design with central point in triplicate to synthesize strontium molybdate by EDTA-citrate combined complexation method, where the influence of pH (6, 7.5 e 9), calcining time (3, 4 e 5 h) and heating rate (5, 7 e 10 °C min−1) was investigated. Single-phase powders were obtained when calcined at 650 °C with tetragonal crystalline structure. The heating rate is the most influent independent variable on the intensities of the X-ray diffractions peaks. The synthesized powders are shown as agglomerates with irregular spherical and bipyramidal morphology. According to the experimental design, the conditions of calcining time of 3 h and heating rate of 10 °C min−1 show the lowest values of energy band gap (4.18 and 4.17 eV) for pH 6 and 9, respectively. The statistical models generated were able to describe the phenomena observed | |
| dc.description | 2029 | |
| dc.language | en | |
| dc.publisher | Elsevier | |
| dc.subject | Strontium molybdate | |
| dc.subject | EDTA-citrate method | |
| dc.subject | Experimental design | |
| dc.subject | Optical bandgap | |
| dc.subject | Morphology | |
| dc.title | Experimental planning of the synthesis of strontium molybdate by EDTA-citrate and its structural influence, morphology and optical bandgap | |
| dc.type | article | |
