masterThesis
Desenvolvimento de pastas leves utilizando microesferas ocas de cerâmica para aplicação em cimentação de poços petrolíferos
Fecha
2022-05-23Registro en:
LIMA, João Afonso Néo de Andrade. Desenvolvimento de pastas leves utilizando microesferas ocas de cerâmica para aplicação em cimentação de poços petrolíferos. 2022. 83f. Dissertação (Mestrado em Engenharia Química) - Centro de Tecnologia, Universidade Federal do Rio Grande do Norte, Natal, 2022.
Autor
Lima, João Afonso Néo de Andrade
Resumen
Geopressures are related to the main problems caused during the drilling of wells, and any
damage caused to the formations can compromise their safety and economy. Therefore,
alternative solutions are needed to control the pressures exerted during the displacement of
cement slurries, such as changing their density. One way to reduce the specific mass of the
slurries is to use light aggregates in their composition, and among these, the hollow ceramic
microsphere has potential for this application. In addition, hollow ceramic microspheres, as they
are by-products of coal burning, have a low cost and are environmentally sustainable. Given
the above, the objective of this work was to develop slurry designs with low specific weight,
using hollow ceramic (fly ash) and silicate microspheres for application in primary cementing
operations of oil wells. The hollow ceramic microspheres were characterized by pycnometer,
granulometric analysis, XRD, and XRF to determine their class according to ASTMC618−12A. The slurry designs were formulated with specific masses between 11.5 lb/gal and
12.5 lb/gal. The tests were carried out using the practical recommendations of API RP 10B-2
and PROCELAB. According to the stability tests, sodium silicate had the most significant
influence on the cohesion of the particles, with a concentration of 0.3 gpc being the most
suitable for systems that contain light aggregates in their composition. The studied systems
showed compressive strength results between 3.0 and 13.5 Mpa in 24 hours of curing,
satisfactory results for slurries with low specific mass, proving the potential of partial
replacement of Portland cement by industrial waste, making its application more sustainable
and less expensive.