Synthesis and characterization of ammonium acesulfamate

dc.creatorEcheverría, Gustavo Alberto
dc.creatorPiro, Oscar Enrique
dc.creatorParajón Costa, Beatriz S.
dc.creatorBarán, Enrique José
dc.date2014
dc.date2019-11-07T16:48:56Z
dc.identifierhttp://sedici.unlp.edu.ar/handle/10915/85161
dc.identifierissn:0932-0776
dc.descriptionAmmonium acesulfamate, (NH4)C4H4NO 4S, was prepared by the reaction of acesulfamic acid and ammonium carbonate in aqueous solution, and characterized by elemental analysis and 1H and 13C NMR spectroscopy. Its crystal and molecular structure was determined by single-crystal X-ray diffraction methods. The substance crystallizes in the orthorhombic space group Pnma with Z = 4 molecules per unit cell. The NH4 + ion generates medium to strong hydrogen bonds with the carbonylic oxygen, the iminic nitrogen and the sulfonyl oxygen atoms of the acesulfamate anion. The FTIR spectrum of the compound was also recorded and is briefly discussed.
dc.descriptionFacultad de Ciencias Exactas
dc.descriptionInstituto de Física La Plata
dc.descriptionCentro de Química Inorgánica
dc.formatapplication/pdf
dc.format737-741
dc.languageen
dc.rightshttp://creativecommons.org/licenses/by-nc-sa/4.0/
dc.rightsCreative Commons Attribution-NonCommercial-ShareAlike 4.0 International (CC BY-NC-SA 4.0)
dc.subjectQuímica
dc.subjectAmmonium Acesulfamate
dc.subjectCrystal Structure
dc.subjectFTIR Spectra
dc.subjectSynthesis
dc.titleSynthesis and characterization of ammonium acesulfamate
dc.typeArticulo
dc.typeArticulo


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