Determination of the sodium monofluoroacetate in serum by gas chromatography

dc.contributorUniversidade do Sagrado Coração (USC)
dc.contributorUniversidade Estadual Paulista (Unesp)
dc.date.accessioned2014-05-20T15:30:39Z
dc.date.available2014-05-20T15:30:39Z
dc.date.created2014-05-20T15:30:39Z
dc.date.issued2001-09-01
dc.identifierChromatographia. Wiesbaden: Vieweg, v. 54, n. 5-6, p. 402-404, 2001.
dc.identifier0009-5893
dc.identifierhttp://hdl.handle.net/11449/39978
dc.identifier10.1007/BF02492692
dc.identifierWOS:000171316600020
dc.identifier4659698040759224
dc.description.abstractSodium monofluoroacetate (NAFAc) has been widely used for vertebrate pest control, such as rabbits in Australia. However NAFAc is extremely toxic to all vertebrates and its use is restricted. Although this compound is stringently restricted, the occurrence of accidental and homicidal poisoning is no ever-present possibility.The method developed in this work shows the applicability of SPE with alumina cartridges for the extraction of NAFAc from serum samples. The method is efficient with recoveries of at least 96.8% from spiked serum. The samples were subsequently derivatized with dicyclohexylcabodiimide (DCC), using 2,4-dichloroaniline (DCA), to make the product volatile for GC analysis.
dc.languageeng
dc.publisherVieweg
dc.relationChromatographia
dc.relation1.401
dc.relation0,514
dc.rightsAcesso restrito
dc.sourceWeb of Science
dc.subjectgas chromatography
dc.subjectsodium monofluoroacetate
dc.subjectrodents
dc.subjectalumina
dc.titleDetermination of the sodium monofluoroacetate in serum by gas chromatography
dc.typeArtículos de revistas


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