Artículos de revistas
Thiosaccharine disulfide: Synthesis, crystal structure, spectroscopic characterization and theoretical study
Fecha
2013-01Registro en:
Ferullo, Ricardo; Granados, Alejandro Manuel; Lanterna, Anabel Estela; Guida, Jorge Alberto; Piro, Oscar Enrique; et al.; Thiosaccharine disulfide: Synthesis, crystal structure, spectroscopic characterization and theoretical study; Elsevier Science; Journal Of Molecular Structure Theochem; 1032; 30; 1-2013; 48-55
0166-1280
Autor
Ferullo, Ricardo
Granados, Alejandro Manuel
Lanterna, Anabel Estela
Guida, Jorge Alberto
Piro, Oscar Enrique
Castellano, Eduardo E.
Dennehy, Mariana
Resumen
The title compound, (thiosaccharine disulfide), bis[1,10dioxide-2,3-dihidro-1,2-benzoisothiazol]disulfide,(tsac)2 has been synthesized and fully characterized by UV?Visible, IR, Raman, 1H and 13C NMR spectroscopy elemental analysis and structural X-ray crystallography. A DFT theoretical study has been performed and good agreement between experimental and theoretical values of structural parameters and vibration frequencies have been achieved.