The influence of crucible material on the DSC thermal analysis compared to freeze-drying microscopy results

dc.creatorTATTINI JR., Virgilio
dc.creatorPARRA, Duclerc Fernandes
dc.creatorPITOMBO, Ronaldo Nogueira de Moraes
dc.date.accessioned2012-10-19T03:18:17Z
dc.date.accessioned2018-07-04T14:56:27Z
dc.date.available2012-10-19T03:18:17Z
dc.date.available2018-07-04T14:56:27Z
dc.date.created2012-10-19T03:18:17Z
dc.date.issued2009
dc.identifierJOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, v.98, n.1, p.203-206, 2009
dc.identifier1388-6150
dc.identifierhttp://producao.usp.br/handle/BDPI/19777
dc.identifier10.1007/s10973-009-0317-8
dc.identifierhttp://dx.doi.org/10.1007/s10973-009-0317-8
dc.identifier.urihttp://repositorioslatinoamericanos.uchile.cl/handle/2250/1616562
dc.description.abstractThe aim of this study was to investigate the influence of different crucible materials on the thermal analysis of binary systems. The thermal properties of two distinct solutions were measured both by Differential Scanning Calorimetry (DSC) and freeze-drying microscopy and the results were compared. The glass transition of the maximally freeze-concentrate (T (g)`) and the eutectic melting temperature (T (eut)) were not influenced by the crucible material. However the heat of fusion (Delta H) involved during the T (eut) as well as the Delta C (p) involved during the T (g)` of the solutions were affected.
dc.languageeng
dc.publisherSPRINGER
dc.relationJournal of Thermal Analysis and Calorimetry
dc.rightsCopyright SPRINGER
dc.rightsrestrictedAccess
dc.subjectLyophilization
dc.subjectEutectic temperature
dc.subjectGlass transition temperature
dc.subjectDifferential scanning calorimetry
dc.subjectFreeze-drying microscopy
dc.titleThe influence of crucible material on the DSC thermal analysis compared to freeze-drying microscopy results
dc.typeArtículos de revistas


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