dc.creatorGalembeck, A
dc.creatorAlves, OL
dc.date2002
dc.dateMAY 15
dc.date2014-11-15T20:17:14Z
dc.date2015-11-26T16:13:43Z
dc.date2014-11-15T20:17:14Z
dc.date2015-11-26T16:13:43Z
dc.date.accessioned2018-03-28T23:01:13Z
dc.date.available2018-03-28T23:01:13Z
dc.identifierJournal Of Materials Science. Kluwer Academic Publ, v. 37, n. 10, n. 1923, n. 1927, 2002.
dc.identifier0022-2461
dc.identifierWOS:000175095300001
dc.identifier10.1023/A:1015206426473
dc.identifierhttp://www.repositorio.unicamp.br/jspui/handle/REPOSIP/55730
dc.identifierhttp://www.repositorio.unicamp.br/handle/REPOSIP/55730
dc.identifierhttp://repositorio.unicamp.br/jspui/handle/REPOSIP/55730
dc.identifier.urihttp://repositorioslatinoamericanos.uchile.cl/handle/2250/1267400
dc.descriptionPolycrystalline bismuth vanadate, BiVO4, was synthesized by metallo-organic decomposition (MOD), starting from bismuth 2-ethyl-hexanoate and vanadium (IV) oxy-acetylacetonate solutions in an organic solvent. The pyrolysis of the precursors at 500degreesC lead to single-phase samples, with particle sizes ranging from 0.65 to 1.40 mum, depending upon the heating time. The activation energies for the thermal decomposition of the precursors were estimated as 100.0 kJ/mol and 90.5 kJ/mol for bismuth and vanadium precursors, respectively. The method allows for the synthesis of powdered polycrystalline and/or thin film samples and may provide a route to doped/substituted compounds with minimal changes in the experimental procedures. (C) 2002 Kluwer Academic Publishers.
dc.description37
dc.description10
dc.description1923
dc.description1927
dc.languageen
dc.publisherKluwer Academic Publ
dc.publisherDordrecht
dc.publisherHolanda
dc.relationJournal Of Materials Science
dc.relationJ. Mater. Sci.
dc.rightsfechado
dc.sourceWeb of Science
dc.subjectThin-films
dc.subjectTemperature
dc.subjectBivo4
dc.subjectSuperconductor
dc.subjectElectrode
dc.subjectMicrowave
dc.titleBismuth vanadate synthesis by metallo-organic decomposition: thermal decomposition study and particle size control
dc.typeArtículos de revistas


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