Determination Of The Phenolic Composition From Brazilian Tropical Fruits By Uhplc-ms/ms

dc.creatorBataglion G.A.
dc.creatorDa Silva F.M.A.
dc.creatorEberlin M.N.
dc.creatorKoolen H.H.F.
dc.date2015
dc.date2015-06-25T12:51:20Z
dc.date2015-11-26T14:58:24Z
dc.date2015-06-25T12:51:20Z
dc.date2015-11-26T14:58:24Z
dc.date.accessioned2018-03-28T22:10:05Z
dc.date.available2018-03-28T22:10:05Z
dc.identifier
dc.identifierFood Chemistry. Elsevier Ltd, v. 180, n. , p. 280 - 287, 2015.
dc.identifier3088146
dc.identifier10.1016/j.foodchem.2015.02.059
dc.identifierhttp://www.scopus.com/inward/record.url?eid=2-s2.0-84923326572&partnerID=40&md5=976557776860d8072b597e7fa8d004a9
dc.identifierhttp://www.repositorio.unicamp.br/handle/REPOSIP/85237
dc.identifierhttp://repositorio.unicamp.br/jspui/handle/REPOSIP/85237
dc.identifier2-s2.0-84923326572
dc.identifier.urihttp://repositorioslatinoamericanos.uchile.cl/handle/2250/1255846
dc.descriptionAlthough Brazil is the third largest fruit producer in the world, several specimens consumed are not well studied from the chemical viewpoint, especially for quantitative analysis. For this reason and the crescent employment of mass spectrometry (MS) techniques in food science we selected twenty-two phenolic compounds with important biological activities and developed an ultra-high performance liquid chromatography tandem mass spectrometry (UHPLC-MS/MS) method using electrospray (ESI) in negative ion mode aiming their quantification in largely consumed Brazilian fruits (açaí-do-Amazonas, acerola, cashew apple, camu-camu, pineapple and taperebá). Multiple reaction monitoring (MRM) was applied and the selection of proper product ions for each transition assured high selectivity. Linearity (0.995 < r2 < 0.999), limit of detection (28.85-333.3 pg/mL), limit of quantification (96.15-1111 pg/mL), inter- and intraday accuracy (>80%), precision (CV < 20%) and extraction recovery rate (>80%) were satisfactory and showed that the method provides an efficient protocol to analyze phenolic compounds in fruit pulp extracts.
dc.description180
dc.description
dc.description280
dc.description287
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dc.languageen
dc.publisherElsevier Ltd
dc.relationFood Chemistry
dc.rightsfechado
dc.sourceScopus
dc.titleDetermination Of The Phenolic Composition From Brazilian Tropical Fruits By Uhplc-ms/ms
dc.typeArtículos de revistas


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