Influence Of The Temperature On The Structure Of An Amorphous Ni 46ti 54 Alloy Produced By Mechanical Alloying

dc.creatorGasperini A.A.M.
dc.creatorMacHado K.D.
dc.creatorBuchner S.
dc.creatorDe Lima J.C.
dc.creatorGrandi T.A.
dc.date2008
dc.date2015-06-30T19:13:01Z
dc.date2015-11-26T14:39:34Z
dc.date2015-06-30T19:13:01Z
dc.date2015-11-26T14:39:34Z
dc.date.accessioned2018-03-28T21:45:20Z
dc.date.available2018-03-28T21:45:20Z
dc.identifier
dc.identifierEuropean Physical Journal B. , v. 64, n. 2, p. 201 - 209, 2008.
dc.identifier14346028
dc.identifier10.1140/epjb/e2008-00312-9
dc.identifierhttp://www.scopus.com/inward/record.url?eid=2-s2.0-52349100684&partnerID=40&md5=21a083e372707b8061303228628ad140
dc.identifierhttp://www.repositorio.unicamp.br/handle/REPOSIP/105280
dc.identifierhttp://repositorio.unicamp.br/jspui/handle/REPOSIP/105280
dc.identifier2-s2.0-52349100684
dc.identifier.urihttp://repositorioslatinoamericanos.uchile.cl/handle/2250/1250055
dc.descriptionThe evolution of the local atomic order of an amorphous Ni 46Ti 54 alloy produced by mechanical alloying as a function of temperature was studied by synchrotron X-ray diffraction (XRD) and differential scanning calorimetry (DSC) techniques. XRD measurements at several temperatures (25 °C, 350 °C, 412 °C, 430 °C, 450 °C and 515 °C) were performed and analyzed using the reverse Monte Carlo (RMC) simulations method or the Rietveld refinement procedure. The experimental total structure factor for samples at 25 °C and 350 °C, which are amorphous in nature, were simulated by using the RMC method, and the local structures of the alloy at both temperatures were determined, indicating a decrease in its density as the temperature increases. At 412 °C, the XRD pattern shows a partially crystalline sample, indicating that the crystallization process is in progress. At 430 °C, 450 °C and 515 °C, the XRD measurements indicate the presence of two crystalline phases, NiTi and NiTi 2, whose structural parameters (lattice parameters, coherently diffracting domains (CDD) sizes, microstrains and relative amount of phases) were determined using the Rietveld refinement procedure. DSC measurements at different heating rates furnished the crystallization temperature, enthalpy and activation energy of the crystallization process, and these values are similar to those found in other amorphous alloys of the Ni-Ti system. They also showed the existence of a second exothermic process, which was related to diffusive processes in the crystalline phases, which could be associated with the changes in the CDD sizes happening from 450 °C to 515 °C. © 2008 Springer-Verlag.
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dc.languageen
dc.publisher
dc.relationEuropean Physical Journal B
dc.rightsfechado
dc.sourceScopus
dc.titleInfluence Of The Temperature On The Structure Of An Amorphous Ni 46ti 54 Alloy Produced By Mechanical Alloying
dc.typeArtículos de revistas


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