Artículos de revistas
Optimization Of Headspace Solid-phase Microextraction Conditions To Determine Fruity-aroma Compounds Produced By Neurospora Sitophila
Registro en:
Analytical Methods. Royal Society Of Chemistry, v. 6, n. 19, p. 7984 - 7988, 2014.
17599660
10.1039/c4ay01111b
2-s2.0-84907156420
Autor
Souza De Carvalho D.
Junior S.B.
Dionisio A.P.
Junior M.M.
Godoy H.T.
Pastore G.M.
Institución
Resumen
The biotechnological production of aromatic compounds is an important alternative to the chemical synthesis of flavor ingredients in food industry. Therefore, the development of an accurate and precise analytical technique for the measurement of the biotechnological production of aromatic compounds is of significant importance. In this paper, we optimize the extraction conditions for headspace solid-phase microextraction coupled to GC-FID and GC-MS for the determination of ethyl hexanoate produced by Neurospora sitophila in a malt-extract medium. Following three SPME fibers were tested: polydimethylsiloxane (PDMS), carboxen-polydimethylsiloxane (CAR/PDMS) and polydimethylsiloxane-divinylbenzene (PDMS/DVB). The PDMS/DVB was the most efficient fiber for trapping the volatile aromatic compound. The optimized SPME extraction temperature and time were 30 °C and 10 min, respectively. This method showed good linearity and the limits of detection (LOD) and limits of quantification (LOQ) of the targeted aromatic compound were 0.6 and 1.9 mg L-1, respectively. The HS-SPME methodology proved to be a simple and rapid approach to quantify ethyl hexanoate accurately and precisely for the biotechnological production process. This journal is 6 19 7984 7988 Soccol, C.R., Medeiros, A.B.P., Vandenberghe, L.P.S., Soares, M., Pandey, A., Production of Aroma Compounds (2008) Current Developments in Solid-state Fermentation, pp. 357-372. , in, Springer Asiatech Publishers Inc., New Delhi Rossi, S.C., Vandenberghe, L.P.S., Pereira, B.M.P., Gago, F.D., Rizzolo, J.A., Pandey, A., Soccol, C.R., Medeiros, A.B.P., (2009) Food Res. Int., 42, pp. 484-486 Bicas, J.L., Silva, J.C., Dionísio, A.P., Pastore, G.M., (2010) Cienc. Tecnol. Aliment., 30, pp. 7-18 Berger, R.G., (2009) Biotechnol. Lett., 31, pp. 1651-1659 Longo, M.A., Sanromán, M.A., (2006) Food Technol. Biotechnol., 44, pp. 335-353 Bicas, J.L., Barros, F.F.C., Wagner, R., Godoy, H.T., Pastore, G.M., (2008) J. Ind. Microbiol. Biotechnol., 35, pp. 1061-1070 Pastore, G.M., Park, Y.K., Min, D.B., (1994) Mycol. Res., 98, pp. 25-35 Pastore, G.M., Park, Y.K., Min, D.B., (1995) Rev. Microbiol., 26, pp. 55-58 Yamauchi, H., Hasuo, T., Amachi, T., Akita, O., Hara, S., Yoshizawa, K., (1989) Agric. Biol. Chem., 53, pp. 1551-1556 Yamauchi, H., Obata, T., Amachi, T., Hara, S., (1991) Agric. Biol. Chem., 55, pp. 3115-3116 Yoshizawa, K., Yamauchi, H., Hasuo, T., Akita, O., Hara, S., (1988) Agric. Biol. Chem., 52, pp. 2129-2130 Bogusz, S., Jr., Melo, A.M.T., Zini, C.A., Godoy, H.T., (2011) J. Chromatogr. A, 1218, pp. 3345-3350 Mokhtari, B., Pourabdollah, K., (2011) Talanta, 87, pp. 118-125 Mokhtari, B., Pourabdollah, K., (2012) J. Inclusion Phenom. Macrocyclic Chem., 74, pp. 183-189 Mokhtari, B., Dalali, N., Pourabdollah, K., (2013) J. Chin. Chem. Soc., 60, pp. 625-631 Mokhtari, B., Dalali, N., Pourabdollah, K., (2013) J. Sep. Sci., 36, pp. 356-361 Mokhtari, B., Dalali, N., Pourabdollah, K., (2013) Chromatographia, 76, pp. 565-570 Mokhtari, B., Dalali, N., Pourabdollah, K., (2012) J. Chil. Chem. Soc., 57, pp. 1428-1431 Pawliszyn, J., (1999) Applications of Solid Phase Microextraction, , RSC, Letchworth Pawliszyn, J., (1997) Solid Phase Microextraction: Theory and Practice, , Wiley-VCH, New York Demyttenaere, J.C.R., Adams, A., Vanoverschelde, J., Kimpe, N., Agric, J., (2008) Food Chem., 56, pp. 3287-3296 Maróstica, M.R., Jr., Mota, N., Baudet, N., Pastore, G.M., (2007) Food Sci. Biotechnol., 16, pp. 37-42 Riu-Aumatell, M., Miró, P., Serra-Cayuela, A., Buxaderas, S., López-Tamames, E., (2014) Food Res. Int., 57, pp. 196-202 Bordiga, M., Piana, G., Coïsson, J.D., Travaglia, F., Arlorio, M., (2014) Int. J. Food Sci. Technol., 49, pp. 787-796 Chen, D., Liu, S.Q., (2014) Int. J. Food Sci. Technol., 49, pp. 521-530 Zheng, J., Liang, R., Wu, C., Zhou, R., Liao, X., (2014) Food Res. Int., 56, pp. 77-84 Manríquez, D.A., Muñoz-Robredo, P., Gudenschwager, O., Robledo, P., Defilippi, B.G., (2014) Postharvest Biol. Technol., 94, pp. 58-65 Antón, M.J., Valles, B.S., Hevia, A.G., Lobo, A.P., (2014) J. Food Sci., 79, pp. 92-S99 Arghini, P.B., Gioia, D.D., Fava, F., Ruzzi, M., (2007) Microb. Cell Fact, 6, pp. 13-20 Li, Y., Peng, X., Chen, H., (2013) J. Biosci. Bioeng., 116 (4), pp. 493-498 Davis, R.H., Perkins, D.D., (2002) Nat. Rev. Genet., 3, pp. 397-403 Mannhaupt, G., Montrone, C., Haase, D., Mewes, H.W., Aign, V., Hoheisel, J.D., Fartmann, B., Schulte, U., (2003) Nucleic Acids Res., 31, pp. 1944-1954