Modificação de um micro-extrator de vidro para pré-enriquecimento de traços de pesticidas organoclorados de água para análise por cromatografia gasosa
Modification of a glass micro-extractor aiming to enrichmentt of traces of water contaminating organochlorinated pesticides and their quantitative gas chromatographic analysis
| dc.creator | Rocha, Eduardo Carasek da | |
| dc.creator | Pini, Glaucia Falleiros | |
| dc.creator | Augusto, Fabio | |
| dc.creator | Valente, Antonio Luiz Pires | |
| dc.date | 1998-02-01 | |
| dc.date | 2014-08-05T19:23:46Z | |
| dc.date | 2015-11-26T11:43:47Z | |
| dc.date | 2014-08-05T19:23:46Z | |
| dc.date | 2015-11-26T11:43:47Z | |
| dc.date.accessioned | 2018-03-28T20:47:30Z | |
| dc.date.available | 2018-03-28T20:47:30Z | |
| dc.identifier | Química Nova. Sociedade Brasileira de Química, v. 21, n. 1, p. 109-113, 1998. | |
| dc.identifier | 0100-4042 | |
| dc.identifier | S0100-40421998000100017 | |
| dc.identifier | 10.1590/S0100-40421998000100017 | |
| dc.identifier | http://dx.doi.org/10.1590/S0100-40421998000100017 | |
| dc.identifier | http://www.scielo.br/scielo.php?script=sci_arttext&pid=S0100-40421998000100017 | |
| dc.identifier | http://www.repositorio.unicamp.br/jspui/handle/REPOSIP/82565 | |
| dc.identifier | http://repositorio.unicamp.br/jspui/handle/REPOSIP/82565 | |
| dc.identifier.uri | http://repositorioslatinoamericanos.uchile.cl/handle/2250/1235415 | |
| dc.description | Two models of a glass micro-extractor were constructed after modification of a model proposed in the literature. The two models were used for the simultaneous extraction and enrichment of organochlorinated pesticides from aqueous matrixes to an organic solution appropriate for the gas chromatographic analysis of the pesticide. It was established that the performance of one of the modified micro-extractors permits the pre-concentration of the pesticides to a level that allow their quantitation at the trace level with electron capture detection. It is thus concluded that the glass micro-extractor is a suitable tool for the sample preparation step in the gas chromatographic analysis of environmental pollutants of the class of pesticides. | |
| dc.description | 109 | |
| dc.description | 113 | |
| dc.description | Fundação de Amparo à Pesquisa do Estado de São Paulo (FAPESP) | |
| dc.description | Conselho Nacional de Desenvolvimento Científico e Tecnológico (CNPq) | |
| dc.language | pt | |
| dc.publisher | Sociedade Brasileira de Química | |
| dc.relation | Química Nova | |
| dc.rights | aberto | |
| dc.source | SciELO | |
| dc.subject | pre-concentration of aqueous samples | |
| dc.subject | organochlorinated pesticide | |
| dc.subject | GC analysis | |
| dc.title | Modificação de um micro-extrator de vidro para pré-enriquecimento de traços de pesticidas organoclorados de água para análise por cromatografia gasosa | |
| dc.title | Modification of a glass micro-extractor aiming to enrichmentt of traces of water contaminating organochlorinated pesticides and their quantitative gas chromatographic analysis | |
| dc.type | Artículos de revistas |