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The Black Polymorph of TTF-CA: TTF Polymorphism and Solvent Effects in Mechanochemical and Vapor Digestion Syntheses, FT-IR, Crystal Packing, and Electronic Structure

Lapidus, Saul H.; Naik, Amit; Wixtrom, Alex; Massa, Nestor Emilio; Ta Phuoc, Vinh; del Campo, Leire; Lebegue, Sebestien; Aygyayn, Jaynos G.; Abdel Fattah, Tarek; Pagola, Silvina (American Chemical Society, 2014-01)

Tetrathiafulvalene-chloranil (TTF-CA) was synthesized by two methods, liquid assisted grinding (LAG) and vapor digestion (VD), which largely reduce the use of reaction solvents. The effects of the small quantities of LAG ...