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Narrow bore post column derivatisation assays via reaction flow chromatography
(Elsevier Science, 2018-11)
This study highlights the capability to conduct a post column derivatisation (PCD) process with a narrow bore, low volume column. A reaction flow (RF) HPLC column (30 mm × 2.1 mm internal diameter (i.d.), 3 μm particle ...
Post-column in-source derivatisation in LC-MS: a tool for natural products characterisation and metabolomics
(John Wiley & Sons Ltd, 2020-09)
Introduction: An efficient characterisation of metabolites is a crucial task in many aspects of basic research, such as the de-replication of crude extracts in natural products chemistry or the tentative identification of ...
Total antioxidant capacity with peak specificity via reaction flow chromatography and the ferric reducing antioxidant power assay
(Springer, 2019-12)
An established ferric reducing antioxidant power (FRAP) assay was optimised by preparation of the derivatisation reagent in 300 mM formate instead of 300 mM acetate conditions, resulting in increased sensitivity signal to ...
Better than bench top. High speed antioxidant screening via the cupric reducing antioxidant capacity reagent and reaction flow chromatography
(Elsevier Science, 2020-01)
This study is based upon a recently established method for quantification of the antioxidant capacity of natural samples via a HPLC separation and a hyphenated selective detection (post-column derivatization with cupric ...
Toxicokinetics and toxicodynamics of gonyautoxins after an oral toxin dose in cats
(2002)
Although the action of Gonyautoxins (GTXs) and Saxitoxin (STX) mechanisms is well known at the molecular level, there are still many unresolved questions associated with the intoxication syndrome in mammals. For example, ...
Saxitoxins and okadaic acid group: accumulation and distribution in invertebrate marine vectors from Southern Chile
(Taylor and Francis Ltd., 2015)
© 2015, © 2015 Taylor & Francis. Harmful algae blooms (HABs) are the main source of marine toxins in the aquatic environment surrounding the austral fjords in Chile. Huichas Island (Aysén) has an history of HABs spanning ...
Métodos analíticos para la determinación de Glifosato en matrices ambientales
(Bogotá - Ciencias - Maestría en Ciencias - QuímicaDepartamento de QuímicaUniversidad Nacional de Colombia - Sede Bogotá, 2020-03-19)
El Glifosato es el herbicida más utilizado y comercializado a nivel mundial usado principalmente para el control de malezas. El uso excesivo y su impacto en el medio ambiente, ha promovido el análisis químico del Glifosato ...