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YPdSn and YPd2Sn: Structure, 89Y solid state NMR and 119Sn Mössbauer spectroscopy
(Academic PressMaryland Heights, 2012-06)
The stannides YPdSn and YPd2Sn were synthesized by high-frequency melting of the elements in sealed tantalum tubes. Both structures were refined on the basis of single crystal X-ray diffractometer data: TiNiSi type, Pnma, ...
Sol-gel preparation of mesoporous Al2O3-SiO2 glasses: structural evolution monitored by solid state NMR
(SpringerNew York, 2014-06)
Glasses along the composition line 0.5Al2O3–xSiO2 (1 ≤ x ≤ 6) were prepared via a novel sol-gel route using tetraethylorthosilicate and aluminum lactate as precursors. The structural evolution from solution to gel to glass ...
Solid state NMR studies and chemical shift calculations of a gold(I) complex with a diphosphacyclobutadiene cobaltate sandwich anion
(ElsevierAmsterdam, 2013-06)
The 31P and 13C solid state nuclear magnetic resonance spectra of a neutral gold(I) complex with bis(diphosphacyclobutadiene) cobaltate anions, [Au{Co(P2C2tPent2)2}2(PMe3)2], are reported. Complete 31P resonance assignments ...
A comparative solid state C-13 NMR and thermal study of CO2 capture by amidines PMDBD and DBN
(Royal Soc Chemistry, 2011-01-01)
The present work shows study of the CO2 capture by amidines DBN and PMDBD using C-13 solid-state NMR and thermal techniques. The solid state C-13 NMR analyses demonstrate the formation of a single PMDBD-CO2 product which ...
A comparative solid state C-13 NMR and thermal study of CO2 capture by amidines PMDBD and DBN
(Royal Soc Chemistry, 2011-01-01)
The present work shows study of the CO2 capture by amidines DBN and PMDBD using C-13 solid-state NMR and thermal techniques. The solid state C-13 NMR analyses demonstrate the formation of a single PMDBD-CO2 product which ...
Lithium dynamics in molybdenum disulfide intercalation compounds studied by nuclear magnetic resonance
(SOCIEDADE BRASILEIRA FISICA, 2006-03)
Cluster architecture and lithium motion dynamics are investigated in nanocomposites formed by the intercalation of lithium and a dialkylamine (diethylamine, dibutylamine and dipentylamine) in molybdenum disulfide by means ...
A Homonuclear Rotational Echo Double-Resonance Method for Measuring Site-Resolved Distance Distributions in I=1/2 Spin Pairs, Clusters, and Multispin Systems
(WILEY-V C H VERLAG GMBHWEINHEIM, 2012)