Results of structural, magnetic and transport properties of magnetic Co/SiO2 discontinuous multi-layers produced by sequential deposition are presented. Transmission electron microscopy (TEM) images show that the samples that are close to metal-insulation transition are composed by a connected network of metallic paths, and display an enhanced Hall Effect. The granular samples are composed by an almost periodic array of Co nanoparticles, and after annealing these samples show a clear evolution in the nanostructure, with increasing average Co grain sizes and decreasing size dispersion. Relationships between the nanostructure and magnetotransport properties are discussed and compared with previous results obtained in cosputtered films. © 2005 Elsevier B.V. All rights reserved.2942206212Abeles, B., Sheng, P., Coutts, M.D., Arie, Y., (1975) Adv. Phys., 24, p. 40Vázquez, M., Hernando, A., (1995) Adv. Mater., 7, p. 1021Herzer, G., (1993) Phys. Scripta T, 49, p. 307Hernando, A., Kulik, T., (1994) Phys. Rev. B, 49, p. 7064Denardin, J.C., Brandl, A.L., Knobel, M., Panissod, P., Pakhomov, A.B., Liu, H., Zhang, X.X., (2002) Phys. Rev. B, 65, p. 064422Milner, A., Gerber, A., Groisman, B., Karpovsky, M., Gladkikh, A., (1996) Phys. Rev. Lett., 76, p. 475Slawska-Waniewska, A., Gutowski, M., Lachowicz, H.K., Kulik, T., Matyja, H., (1992) Phys. Rev. B, 46, p. 14594Pakhomov, A.B., Yan, X., Zhao, B., (1995) Appl. Phys. Lett., 67, p. 3497Jing, X.N., Wang, N., Pakhomov, A.B., Fung, K.K., Yan, X., (1996) Phys. Rev. B, 53, p. 14032Denardin, J.C., Knobel, M., Pakhomov, A.B., Zhang, X.X., (2003) J. Magn. Magn. Mater., 262, p. 15Aronzon, B.A., Rylkov, V.V., Kovalev, D.Y., Meilikhov, E.Z., Ryl'Kov, V.V., Sedova, M.V., (2000) Phys. Stat. Solidi, 218, p. 169Aronzon, B.A., Granovskii, A.B., Kovalev, D.Y., Meilikhov, E.Z., Ryl'Kov, V.V., Sedova, M.V., (2000) JETP Lett., 71, p. 469Zhang, X.X., Wan, C.C., Liu, H., Li, Z.Q., Sheng, P., Lin, J.J., (2001) Phys. Rev. Lett., 86, p. 5562Wan, C.C., Sheng, P., (2002) Phys. Rev. B, 66, p. 075309Maurice, J.L., Briatico, J., Carrey, J., Petroff, F., Schelp, L.F., Vaures, A., (1999) Philos. Mag. A, 79, p. 2921Skumryev, V., Stoyanov, S., Zhang, Y., Hadjipanayis, G., Givord, D., Nogues, J., (2003) Nature, 423, p. 850L.M. Socolovsky, C.L.P. Oliveira, J.C. Denardin, M. Knobel, I.L. Torriani, unpublishedDa Silva, F.C.S., Ferrari, E.F., Knobel, M., (1998) J. Appl. Phys., 84, p. 5366Denardin, J.C., Knobel, M., Socolovsky, L.M., Brandl, A.L., Zhang, X.X., (2003) IEEE Trans. Magn., 39, p. 2767