Low-temperature synthesis of nanosized bismuth ferrite by the soft chemical method

dc.contributorUniversidade Estadual Paulista (UNESP)
dc.creatorAguiar, E. C.
dc.creatorRamirez, M. A.
dc.creatorMoura, F.
dc.creatorVarela, José Arana
dc.creatorLongo, Elson
dc.creatorSimões, A. Z.
dc.date2014-05-27T11:27:28Z
dc.date2016-10-25T18:40:53Z
dc.date2014-05-27T11:27:28Z
dc.date2016-10-25T18:40:53Z
dc.date2013-01-01
dc.date.accessioned2017-04-06T02:07:03Z
dc.date.available2017-04-06T02:07:03Z
dc.identifierCeramics International, v. 39, n. 1, p. 13-20, 2013.
dc.identifier0272-8842
dc.identifierhttp://hdl.handle.net/11449/74162
dc.identifierhttp://acervodigital.unesp.br/handle/11449/74162
dc.identifier10.1016/j.ceramint.2012.06.014
dc.identifierWOS:000315246300002
dc.identifier2-s2.0-84869082046
dc.identifier2-s2.0-84862311293
dc.identifierhttp://dx.doi.org/10.1016/j.ceramint.2012.06.014
dc.identifier.urihttp://repositorioslatinoamericanos.uchile.cl/handle/2250/894935
dc.descriptionThis paper describes research on a simple low-temperature synthesis route to prepare bismuth ferrite nanopowders by the polymeric precursor method using bismuth and iron nitrates. BiFeO 3 (BFO) nanopowders were characterized by means of X-ray diffraction analyses, (XRD), Fourier transform infrared (FT-IR) spectroscopy, Raman spectroscopy (Raman), thermogravimnetric analyses (TG-DTA), ultra-violet/vis (UV/Vis) and field emission scanning electron microscopy (FE-SEM). XRD patterns confirmed that a pure perovskite BiFeO 3 structure with a rhombohedral distorted perovskite structure was obtained by heating at 850 °C for 4 hours. Typical FT-IR spectra for BFO powders revealed the formation of a perovskite structure at high temperatures due to a metal-oxygen bond while Raman modes indicated oxygen octahedral tilts induced by structural distortion. A homogeneous size distribution of BFO powders obtained at 850 °C for 4 hours was verified by FE-SEM analyses. © 2012 Elsevier Ltd and Techna Group S.r.l.
dc.languageeng
dc.relationCeramics International
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectA. Ceramics
dc.subjectB. Chemical syntheses
dc.subjectB. Powder metallurgy
dc.subjectC. X-Ray diffraction
dc.subjectBismuth ferrites
dc.subjectChemical synthesis
dc.subjectField emission scanning electron microscopy
dc.subjectFourier transform infrared
dc.subjectFT-IR spectrum
dc.subjectHigh temperature
dc.subjectIron nitrates
dc.subjectLow temperature synthesis
dc.subjectMetal-oxygen bonds
dc.subjectNano powders
dc.subjectPerovskite structures
dc.subjectPolymeric precursor methods
dc.subjectRaman modes
dc.subjectSoft chemical method
dc.subjectStructural distortions
dc.subjectUltra-violet
dc.subjectXRD
dc.subjectXRD patterns
dc.subjectBismuth
dc.subjectFerrite
dc.subjectField emission microscopes
dc.subjectIron research
dc.subjectLow temperature effects
dc.subjectNanostructured materials
dc.subjectOxygen
dc.subjectPerovskite
dc.subjectPowder metallurgy
dc.subjectPowder metals
dc.subjectRaman spectroscopy
dc.subjectTemperature
dc.subjectX ray diffraction
dc.subjectX ray diffraction analysis
dc.subjectBismuth compounds
dc.titleLow-temperature synthesis of nanosized bismuth ferrite by the soft chemical method
dc.typeOtro


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