Otro
High-resolution thermal expansion measurements under helium-gas pressure
Registro en:
Review of Scientific Instruments, v. 83, n. 8, 2012.
0034-6748
10.1063/1.4747272
2-s2.0-84865752762.pdf
2-s2.0-84865752762
Autor
Manna, Rudra Sekhar
Wolf, Bernd
De Souza, Mariano
Lang, Michael
Resumen
We report on the realization of a capacitive dilatometer, designed for high-resolution measurements of length changes of a material for temperatures 1.4K ≤ T ≤ 300K and hydrostatic pressure P ≤ 250MPa. Helium ( 4He) is used as a pressure-transmitting medium, ensuring hydrostatic-pressure conditions. Special emphasis has been given to guarantee, to a good approximation, constant-pressure conditions during temperature sweeps. The performance of the dilatometer is demonstrated by measurements of the coefficient of thermal expansion at pressures P ≃ 0.1MPa (ambient pressure) and 104MPa on a single crystal of azurite, Cu 3(CO 3) 2(OH) 2, a quasi-one-dimensional spin S = 1/2 Heisenberg antiferromagnet. The results indicate a strong effect of pressure on the magnetic interactions in this system. © 2012 American Institute of Physics.
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