doctoralThesis
Estudo das ligas titânio-zircônio resultantes do processo de fundição plasma-skull para aplicações como biomateriais
Fecha
2007-07-06Registro en:
MONTENEGRO, Ieda Nadja Silva. Estudo das ligas titânio-zircônio resultantes do processo de fundição plasma-skull para aplicações como biomateriais. 2007. 154 f. Tese (Doutorado em Físico-Química; Química) - Universidade Federal do Rio Grande do Norte, Natal, 2007.
Autor
Montenegro, Ieda Nadja Silva
Resumen
The aim of this work was to study a series of 11 different compositions of Ti-Zr binary alloys resistance to aggressive environment, i. e., their ability to keep their surface properties and mass when exposed to them as a way to evaluate their performance as biomaterials. The first stage was devoted to the fabrication of tablets from these alloys by Plasma-Skull casting method using a Discovery Plasma machine from EDG Equipamentos, Brazil. In a second stage, the chemical composition of each produced tablet was verified. In a third stage, the specimen were submitted to: as-cast microstructure analysis via optical and scanning electron microscopy (OM and SEM), x-ray dispersive system (EDS) chemical analysis via SEM, Vickers hardness tests for mechanical evaluation and corrosion resistence tests in a 0.9% NaCl solution to simulate exposition to human saliva monitored by open circuit potential and polarization curves. From the obtained results, it was possible to infer that specimens A1 (94,07 wt% Ti and 5,93% wt% Zr), A4 (77,81 wt % Ti and 22,19 wt % Zr) and A8 (27,83 wt% Ti and 72,17 wt% Zr), presented best performance regarding to corrosion resistance, homogeneity and hardness which are necessary issues for biomaterials to be applied as orthopedic and odontological prosthesis