Artículos de revistas
Quantificação do linalol no óleo essencial da Aniba duckei Korstermans utilizando uma nova coluna capilar POLYH4-MD em Cromatografia Gasosa
Fecha
2003-08-01Registro en:
Química Nova. Sociedade Brasileira de Química, v. 26, n. 4, p. 461-465, 2003.
0100-4042
10.1590/S0100-40422003000400002
S0100-40422003000400002
S0100-40422003000400002.pdf
3612277056838097
Autor
Universidade de São Paulo (USP)
Universidade Estadual Paulista (Unesp)
Universidade Federal do Amazonas (UFAM)
Universidade Federal do Maranhão (UFMA)
Institución
Resumen
In the present work a polyurethane polymer derived from castor oil was used as stationary phase for capillary gas chromatography. The polymer was obtained by reaction of hydroxylated compound and isocynate (NCO), forming urethane. Columns of 7 m x 0,25 mm were then coated with this stationary phase (film thickness of 0,25 µm) using static coating method. The Grob test was also performed. Samples of essential oil of the Aniba duckei Korstermans was then analysed in POLYH4-MD capillary column in order to evaluate its chromatographic perfomance. The linalool was found to be the major component and has been used as compound of departure for many important syntheses. Results show that the experimental columns give higher resolution and can be employed for analysis of essentials oils.