HPLC determination of pesticides in soybeans using matrix solid phase dispersion

dc.creatorMaldaner, L
dc.creatorSantana, CC
dc.creatorJardim, ICSF
dc.date2008
dc.date2014-11-14T14:30:21Z
dc.date2015-11-26T17:15:21Z
dc.date2014-11-14T14:30:21Z
dc.date2015-11-26T17:15:21Z
dc.date.accessioned2018-03-29T00:03:36Z
dc.date.available2018-03-29T00:03:36Z
dc.identifierJournal Of Liquid Chromatography & Related Technologies. Taylor & Francis Inc, v. 31, n. 7, n. 972, n. 983, 2008.
dc.identifier1082-6076
dc.identifierWOS:000253506700004
dc.identifier10.1080/10826070801924675
dc.identifierhttp://www.repositorio.unicamp.br/jspui/handle/REPOSIP/68876
dc.identifierhttp://www.repositorio.unicamp.br/handle/REPOSIP/68876
dc.identifierhttp://repositorio.unicamp.br/jspui/handle/REPOSIP/68876
dc.identifier.urihttp://repositorioslatinoamericanos.uchile.cl/handle/2250/1282027
dc.descriptionA method to determine six pesticides applied in soy cultivation (imazethapyr, imazaquin, metsulfuron-methyl, carboxin, chlorimuron-ethyl, and tebuconazole) using matrix solid phase dispersion (MSPD) as the extraction technique followed by a clean-up step, using a C8 co-column, and subsequent chromatographic analysis by high performance liquid chromatography diode array detection (HPLC-DAD) was developed. The validated method showed good recuperation for all pesticides (60-120%), except for metsulfuron-methyl and tebuconazole at their lowest concentration levels, and the quantification limits of the method (0.04-0.08gg-1) were below the maximum residue limits imposed by the principal regulatory agencies.
dc.description31
dc.description7
dc.description972
dc.description983
dc.languageen
dc.publisherTaylor & Francis Inc
dc.publisherPhiladelphia
dc.publisherEUA
dc.relationJournal Of Liquid Chromatography & Related Technologies
dc.relationJ. Liq. Chromatogr. Relat. Technol.
dc.rightsfechado
dc.rightshttp://journalauthors.tandf.co.uk/permissions/reusingOwnWork.asp
dc.sourceWeb of Science
dc.subjectsoy
dc.subjectmulticlass pesticides analysis
dc.subjectsample preparation
dc.subjectMSPD
dc.subjectmethod validation
dc.subjectHPLC-DAD
dc.subjectMass-spectrometry
dc.subjectExtraction Techniques
dc.subjectResidues
dc.subjectFood
dc.subjectEnvironment
dc.titleHPLC determination of pesticides in soybeans using matrix solid phase dispersion
dc.typeArtículos de revistas


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